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، جلد ۶، شماره ۴، صفحات ۳۰۳-۳۱۲
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| عنوان فارسی |
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| چکیده فارسی مقاله |
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| کلیدواژه‌های فارسی مقاله |
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| عنوان انگلیسی |
Response Surface Methodology for Optimization of Supercritical Fluid Extraction of Orange Peel Essential Oil |
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| چکیده انگلیسی مقاله |
Background: Orange peel essential oils were obtained using supercritical fluid extraction. This method is an important high scaling extraction method used for the extraction of plant and animal extracts. Objectives: The aim of this study was the optimization of the extraction of the orange peel essential oil. Methods: The experimental parameters of Supercritical Fluid Extraction (SFE) such as temperature, pressure, and extraction time, and modifier volume were optimized using a central composite design after a 24-1 fractional factorial design. Orange peels were collected from ripe orange and were washed, air dried, and milled. Then, a Suprex MPS/225 system in the SFE mode with a maximal operating pressure of 395 bars was used for essential oil extraction. Moreover, GC-MS and GC-FID were used for the identification and determination of oil compounds, respectively. Results: Eight compounds have been identified based on their retention indices and mass spectra. According to the results, α-pinene, β-pinene, myrcene, d-limonene, terpinolene, C8-aldehyde, citronellol, and linalool were identified in orange peel essential oil. The optimum SFE conditions were obtained at a pressure of 347.07 atm, temperature of 55° C, extraction time of 30.16 min, and ethanol volume of 147.05 µL. Moreover, extraction yields based on SFE varied in the range of 0.04% to 1.18% (w/w). Conclusion: The Results showed supercritical fluid technology as the best alternative technique for the extraction of pure and high-quality essential oil from orange peel. It is a green method and does not have any environmental impact. |
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| کلیدواژه‌های انگلیسی مقاله |
Essential oils, Extraction, Supercritical fluid extraction, Volatile compounds |
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| نویسندگان مقاله |
| Kiana Ghadiri
Active Pharmaceutical Research Center (APIRC), Pharmaceutical Science Branch, Islamic Azad University, Tehran, Iran.
| Farhad Raofie
Department of Chemistry, Faculty of Science, Shahid Beheshti University, Tehran, Iran.
| Mahnaz Qomi
Active Pharmaceutical Research Center (APIRC), Pharmaceutical Science Branch, Islamic Azad University, Tehran, Iran.
| Ali Davoodi
Department of Pharmacognosy and Biotechnology, Faculty of Pharmacy, Mazandaran University of Medical Sciences, Sari, Iran.
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| نشانی اینترنتی |
http://pbr.mazums.ac.ir/browse.php?a_code=A-10-64-2&slc_lang=en&sid=1 |
| فایل مقاله |
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| کد مقاله (doi) |
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| زبان مقاله منتشر شده |
en |
| موضوعات مقاله منتشر شده |
فارماکوگنوزی |
| نوع مقاله منتشر شده |
پژوهشی |
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